1.
Organic Syntheses Prep
Vol. 6, p.232 (1988); Vol. 55, p.96 (1976). PHASE-TRANSFER HOFMANN CARBYLAMINE REACTION: tert-BUTYL ISOCYANIDE. [Propane, 2-isocyano-2-methyl-] ...
2.
Organic Syntheses Prep
... 17 mm OD Vigreaux column and short path distillation apparatus (18 mm (length) ... flow rate (He) of 1.0 mL/min, and a column gradient from 50 °C for 30 ...
3.
PERBENZOIC ACID
The aqueous solution contains the sodium salt of perbenzoic acid. The perbenzoic acid is liberated by the addition of 225 cc. of cold 1 N sulfuric acid and ...
4.
ASYMMETRIC HYDROBORATION OF 5-SUBSTITUTED CYCLOPENTADIENES ...
Org. Synth., Coll. Vol. V 1973, 976. The checkers also examined the use of .... This preparation is referenced from: Org. Syn. Coll. Vol. 9, 186 ...
5.
PALLADIUM(0)-CATALYZED syn-1,4-ADDITION OF CARBOXYLIC ACIDS TO ...
See Org. Synth., Coll. Vol. V, 1973, 976 for possible hazard. .... Korach, M.; Nielson, D. R.; Rideout, W. H. Org. Synth., Coll. Vol. V, 1973, 414–418. ...
6.
SYNTHESIS OF 4-, 5-, and 6-METHYL-2,2'-BIPYRIDINE BY A NEGISHI ...
4-Methyl-2,2'-bipyridine: 2,2'-Bipyridine, 4-methyl- (9); (56100-19-7). 6-Methyl-2,2'-bipyridine: 2,2'-Bipyridine, 6-methyl- (9); (56100-22-2) ...
7.
PHENYLGLYOXAL
6. The potassium should be free of oxide and/or hydroxide to avoid subsequent saponification of ethyl ... nitrogen (7727-37-9). nitrous acid (7782-77-6) ...
8.
TRICARBALLYLIC ACID
Tricarballylic acid is readily soluble in water (requiring about twice its weight at room temperature), but may, if desired, be recrystallized from it. ...
9.
SYNTHESIS OF EPOXIDES USING DIMETHYLDIOXIRANE: trans-STILBENE OXIDE
13. trans-Stilbene oxide has the following properties: 1H NMR (300 MHz, CDCl3) δ: 3.86 (s, 2 H, 2 × -CH-), 7.26–7.45 (m, 10 H, 2 × C6H5-); 13C NMR (75 MHz, ...
10.
2-(N-BENZYL-N-MESITYLENESULFONYL)AMINO-1-PHENYL-1-PROPYL PROPIONATE
Hexane (100 mL) is added in portions with swirling to the dichloromethane ... C. 2-(N-Benzyl-N-mesitylenesulfonyl)amino-1-phenyl-1-propyl propionate , 1 . ...
